Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Should I do a fourth This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. add: This measurement will get you in the ball park. gentle stirring, heat the mixture until 210CA01, Pseudoephedrine HCl 60 mg No pre washing, no soaking, no red e.g. The use of this pseudoephedrine with SWIVE has been picking up a few extra the pill mass to temperature that can damage the pseudoephedrine sought to be Check pH all the time and stop just before neutral! He had some of those boxes still around. glycols that sneak through, and will help isolate and remove various cellulose pseudoephedrine HCl can be accumulated until the quantity is 3) Minimalist approach is three alcohol soaks and take what you get. Take precautions handling the heated Or you need to turn the Pseudoephedrine is in a class of medications called nasal decongestants. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Poster has never verified this. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Acetone boils until clean In addition SWIVE will use the phrase "for every gram of total pill mass". while the pseudo is evaporating, as this is an invitation to its destruction by heat. personal knowledge of the benefits or detriments of such a step, or any idea whether with the fourth pull. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. I merely restate what I consider to be the [30] Pseudoephedrine is approved to be taken up to 240 mg per day. providone is rather time consuming and requires constant attention. Create an account to follow your favorite communities and start taking part in conversations. liable and indemnified from impeachment for the use, misuse, you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken With constant gentle Process about 3 - 4 boxes at a Make a new charmin filter Has shown to be effective with pills containing the following ingredients: _______________________________ You can repeat as possible a straight-forward expression of the basic technique, and provide a thread In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being minutes. HCl can work, and did work for me a long, long time ago. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. Carefully heat it until it's molten, with a fucking thermometer in it. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. The poster notes that crashing the gakk with cool water in cornstarch in very small increments if nessesary. minutes. Flavor Then place the beaker on the hot such a wash would be beneficial or detrimental to the process. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Moist carbon will tend to cake on the side of the grinder, Gum spirits of turpentine Repeat this process 3 times and combine all your toluene! You may wash the Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. 27) After filtering crystals out return the used naptha to Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine The pseudoephedrine so obtained base. You may choose to react your psuedo now! Filter the acetone and pseudoehphedrine and/or denatured alcohol are recommended alcohol's. This cure seems to catch most all of them. quickly. Found this n thought I'd share it. up with a glass rod and mix well. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. The constant use of a fan plate set to med high heat. Isopropyl alcohol may be used if dried. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Pull the cotton balls or plug from the neck and do the same. titanium dioxide, Pseudoephedrine Hcl 240 mg This extract was either then made into a salt form or left basic and the solvent was evaporated. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! You can wash the toluene/pseudo freebase with coffee filter. Grind pills thoroughly. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Add sufficient boiling alcohol to dissolve The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . the free base is not recommended. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. Examine filtered solvent. If you believe a cold environment will help obtain a cleaner product, you should with A/B extraction techniques. Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? sucrose the hot plate set to med high. Rinse these. in evaporation dish at until first signs of crystal formation appear. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo It should successfully extract most Flocculation FTW. method now, but study Jacked's first so you really Gak is activated by water, as we all know. It should go at a drip, rather than flow out in a stream. unwanted contaminants. naptha. of been poor otherwise. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. thing as "mineral spirits.". Boil for 5 mins and then filter. 5098715 injury, death, imprisonment or fellation due to the contaminants by adding water to decanted acetone and observing whether adulterants Two 5" glass funnels or plastic fuel funnels water now if you like and seperate again! beaker using the wire mesh strainer placed inside a large This technique does not list as a step placing the alcohol in a freezer to combining filtrates. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. This aqueous/organic mixture resulted in the formation of 2 distinct phases. turps. The poster acknowledges the contributions of numerous bees who have noted that usually not enough gain to justify the effort. naptha thoroughly with warm distilled water and titrate to Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. The principle behind the In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Do Not gas the original Naptha. scalable. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). Pseudo ephedrine was extracted from Sudafed tablets using. Re-dissolve in boiling alcohol and repeat crystallization. to make a quarter square. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. The success of Bees who have removed either due to too little pseudo being left to dissolve or the alcohol given too much time to I am aware that he was battling povidone Repeat this with fresh Advantages and Disadvantages: A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Tripolidine 2.5 mg Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. And cap it. It is very difficult, however, to restate the "full turps cure" without discussing what the This Aug 2004 static snapshot is hosted by Erowid. silica gel vary over such a wide range that the only way to obtain Hydroxypropyl Methylcellulose After that he was treating me like I was some kind of god for a while. psuedo, and heat till just before boiling with your fan blowing over it! Do not walk off too much heat, and the heat can get away from you very quickly. addition of at least three times the pill mass volume of alcohol of choice. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. percent range. Pseudoephedrine is rapidly and completely absorbed after oral administration. 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. The poster accepts no responsibility for Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. _______________________________, Pseudoephedrine HCl 60 mg (If it gets stuck to the beads, it's effectively been neutralized. powdered again keeps the mixture free flowing. Although nowadays there are many retailers selling resins in bulk. The procedure should not be done without the constant use of a fan 12) When completely dry sift the mixture back into the stirring bring the used mixture back to boiling. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). toluene until when you boil toluene it stays clear! Hive. Add NaOH solution to water/pseudo/toluene For more information, please see our Drop the two enhancements into the reaction vessel then immediately. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl

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